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Volume 4, Issue 4 (Winter 2021)
Abstract

Research subject: Saponin compounds have been considered as anti-cancer, antimicrobial, antifungal, anti-inflammatory, and antiviral activity agents. In addition, they are also used as foaming agents in some food industries. There are few studies for assessing the extraction of this substance, so far. The main purpose of this study is to assess and compare the extraction yield of Saponin by conventional extracting using solvent and super-critical fluid method.
Research approach: In the extraction with solvent, the effect of three independent parameters including mass of solid material, percentage of ethanol solvent, and time of extraction on process performance was investigated. Yield of extraction and Saponin concentration were considered as indexes for evaluating the process performance. In the super critical fluid extraction, the effects of extraction time, pressure, and temperature were investigated. In this method, carbon dioxide was used as super critical fluid and 80% ethanol was used as co-solvent. In order to design of experiment and process optimization, response surface methodology and central composite design was used.
Main results: In optimum condition of extraction with solvent, the mass of solid material, ethanol solvent percentage, and extraction time were 5.4 g, 77.5%, and 7 h, respectively. In this condition, the maximum efficiency of extraction yield of 1.12 mg of saponins per a gram of dry primary substance was obtained. The results indicated that time and solvent percentage were significant parameters.  Further, interaction between two factors of time and solvent percentage was significant. For supercritical fluid extraction, in optimum condition, extraction time, pressure, and temperature were 10 h, 400 bar, and 50 °C, respectively. Extraction yield in this condition was 20% more than the yield of conventional method. It is concluded that the supercritical fluid extraction method has higher performance than conventional method.

Volume 16, Issue 94 (December 2019)
Abstract

Drying foods, such as freezing methods and hot air, are not ideal and reduces the nutritional value and is also expensive and is used only for high value food. In this research, drying with supercritical fluid of carbon dioxide was investigated to remove moisture from the figs. In the drying process with supercritical fluid, the structure of food products is maintained during drying. The design of the experiment was carried out in a factorial arrangement using Design Expert software and analysis variance table to determine the effect of three pressure parameters, temperature, and time to measure the removal rate of moisture. The calculated factorial model was meaningful and able to select the best drying parameters. In optimum conditions, the highest yield (78.109%) with the desirability of 0.992 at 20 MPa, 60 °C and 120 minutes duration. The results showed that the drying of figs during the whole drying period is carried out at the downstream stage, which indicates that the drying of these materials, the internal moisture control, controls the rate of drying and mass transfer. In this study, by solving the second Fick's law and in the range of pressure and temperature tested, with the assumption of the spherical of the fig using the Crank equation, the amount of moisture diffusion coefficient between 4.51× 10-10 and 0.18 × 10 -10 m2/s were obtained. The fig's drying rate was also calculated. Increasing temperature and pressure caused to increase the drying rate.


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